1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

Base Information

Chemical Name:1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol
CAS No.:1446098-88-9
Molecular Formula:C₇₈H₁₂₇NO₁₀
Molecular Weight:1238.87
Hs Code.:

Synonyms:1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

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Chemical Property of 1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

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Technology Process of 1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

There total 28 articles about 1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 3-O-(6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

: 112-67-4
n-hexadecanoyl chloride

: 1446098-88-9
1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

Guidance literature:: With pyridine; dmap; at 20 ℃; for 4h;
DOI:10.1016/j.carres.2013.02.008

Reference yield:

: 1152-39-2,28244-98-6,121523-95-3,131488-68-1
p-methylphenyl-1-thio-β-D-galactopyranoside

: 1446098-88-9
1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; pyridine / 5 h / 80 °C

2.1: sodium hydride / N,N-dimethyl-formamide / 6 h / 0 - 20 °C

3.1: acetic acid / ethanol / 16 h / 90 °C

4.1: dmap; triethylamine / dichloromethane / 5 h / 20 °C

5.1: sodium azide / N,N-dimethyl-formamide / 65 °C

6.1: N-Bromosuccinimide / acetone; water / 20 °C

6.2: 4 h / 0 °C

7.1: trimethylsilyl trifluoromethanesulfonate / diethyl ether / 0.5 h / 0 °C / Molecular sieve

8.1: toluene-4-sulfonic acid / 2 h / 2 °C

9.1: water; triphenylphosphine / tetrahydrofuran / 5 h / 50 °C

10.1: dmap; pyridine / 4 h / 20 °C

With pyridine; dmap; N-Bromosuccinimide; sodium azide; trimethylsilyl trifluoromethanesulfonate; water; sodium hydride; toluene-4-sulfonic acid; acetic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; 9.1: |Staudinger Azide Reduction;
DOI:10.1016/j.carres.2013.02.008

Reference yield:

: C₃₀H₃₅N₃O₇

: 1446098-88-9
1,2-dipalmitoyl-3-(N-palmitoyl-6'-amino-2',3',4'-tri-O-benzyl-6'-deoxy-α-D-galactosyl)-sn-glycerol

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide / 4 h / 50 °C

2: triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

3: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / 40 h / 20 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/j.ejmech.2012.06.007