N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine

Base Information

Chemical Name:N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine
CAS No.:244244-24-4
Molecular Formula:C₂₆H₂₅ClN₂O₃
Molecular Weight:448.949
Hs Code.:

Synonyms:N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine

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Chemical Property of N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine

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Technology Process of N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine

There total 2 articles about N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.4%

: 609-65-4
o-chlorobenzoyl chloride

: 212709-84-7
N-tert-butyl-N'-(9-fluorenylmethoxycarbonyl) hydrazine

: 244244-24-4
N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine

Guidance literature:: With triethylamine; In diethyl ether;
DOI:10.1002/(SICI)1096-9063(199909)55:9<909::AID-PS34>3.0.CO;2-G

Reference yield:

: 82911-69-1
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

: 244244-24-4
N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 83.6 percent / sodium bicarbonate / H₂O; dioxane / 20 °C

2: 86.4 percent / triethylamine / diethyl ether

With sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; diethyl ether; water; 1: Acylation / 2: Acylation;
DOI:10.1002/(SICI)1096-9063(199909)55:9<909::AID-PS34>3.0.CO;2-G

Reference yield: 81.5%

: 244244-24-4
N-tert-butyl-N-(2-chlorobenzoyl)-N'-(9-fluorenylmethoxycarbonyl)hydrazine

: 112225-90-8
N-tert-butyl-N-(2-chlorobenzoyl)hydrazine

Guidance literature:: With piperidine; In N,N-dimethyl-formamide; at 20 ℃; for 9h;
DOI:10.1002/(SICI)1096-9063(199909)55:9<909::AID-PS34>3.0.CO;2-G