11-{[2-(2-{[(10-Ethoxycarbonyldecyl)methylcarbamoyl]methoxy}ethoxy)ace tyl]methylamino}-undecanoic acid, ethyl ester

Base Information

• Chemical Name: 11-{[2-(2-{[(10-Ethoxycarbonyldecyl)methylcarbamoyl]methoxy}ethoxy)ace tyl]methylamino}-undecanoic acid, ethyl ester
• CAS No.: 38252-51-6
• Molecular Formula: C₃₄H₆₄N₂O₈
• Molecular Weight: 628.891
• Mol file: 38252-51-6.mol

Synonyms:15,18-Dioxa-12,21-diazadotriacontanedioicacid, 12,21-dimethyl-13,20-dioxo-, diethyl ester (9CI)

Chemical Property of 11-{[2-(2-{[(10-Ethoxycarbonyldecyl)methylcarbamoyl]methoxy}ethoxy)ace tyl]methylamino}-undecanoic acid, ethyl ester

Chemical Property:

• PSA: 120.47000
• LogP: 6.17560

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 11-{[2-(2-{[(10-Ethoxycarbonyldecyl)methylcarbamoyl]methoxy}ethoxy)ace tyl]methylamino}-undecanoic acid, ethyl ester

There total 1 articles about 11-{[2-(2-{[(10-Ethoxycarbonyldecyl)methylcarbamoyl]methoxy}ethoxy)ace tyl]methylamino}-undecanoic acid, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,6-dioxa-1,8-octanoyl dichloride (31255-09-1) + ethyl 11-methylaminoundecanoate (51227-19-1) → 11-{[2-(2-{[(10-Ethoxycarbonyl-decyl)-methyl-carbamoyl]-methoxy}-ethoxy)-acetyl]-methyl-amino}-undecanoic acid ethyl ester (38252-51-6)

Guidance literature:

With pyridine; In diethyl ether;

DOI:10.1002/hlca.19730560538

Reference yield:

11-{[2-(2-{[(10-Ethoxycarbonyl-decyl)-methyl-carbamoyl]-methoxy}-ethoxy)-acetyl]-methyl-amino}-undecanoic acid ethyl ester (38252-51-6) + N,N-dimethylformamide dibenzyl acetal (2016-04-8) → 11-{[2-(2-{[(10-Benzyloxycarbonyl-decyl)-methyl-carbamoyl]-methoxy}-ethoxy)-acetyl]-methyl-amino}-undecanoic acid benzyl ester (43133-04-6)

Guidance literature:

Multistep reaction; (i) aq. K₂CO₃, EtOH, (ii) /BRN= 2052397/, CHCl₃;

DOI:10.1002/hlca.19730560538

upstream raw materials:

3,6-dioxa-1,8-octanoyl dichloride

ethyl 11-methylaminoundecanoate

Downstream raw materials:

11-{[2-(2-{[(10-Benzyloxycarbonyl-decyl)-methyl-carbamoyl]-methoxy}-ethoxy)-acetyl]-methyl-amino}-undecanoic acid benzyl ester

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