(4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene

Base Information

Chemical Name:(4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene
CAS No.:1181274-23-6
Molecular Formula:C₃₀H₂₁N₂O₃P
Molecular Weight:488.482
Hs Code.:

Synonyms:(4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene

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Chemical Property of (4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene

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Technology Process of (4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene

There total 1 articles about (4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 137156-22-0,171878-71-0,155613-52-8
binaphthol chlorophosphite

: 123532-18-3
3-(2-hydroxyphenyl)-1-methyl-1H-pyrazole

: 1181274-23-6
(4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1039/b822144h

Reference yield: 85.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 1181274-23-6
(4-(2-(1-methyl-1H-pyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a;3,4-a']dinaphtalene

: 1180605-29-1
dichlorido[(η6-para-cymene)(4-(2-(1-methylpyrazol-3-yl))phenyloxy)-3,5-dioxa-4-phosphacyclohepta[2,1-a:3,4-a']dinaphthalene]ruthenium(II)

Guidance literature:: In dichloromethane; (under N2); soln. of ligand in CH2Cl2 added to soln. of Ru-complex in CH2Cl2, stirred for 24 h at room temp.; solvent reduced, Et2O added, filtered, washed with Et2O, recrystd. from toluene/THF; elem. anal.;
DOI:10.1039/b822144h