2-phenyl-1-isobutylcycloethylimine

Base Information

• Chemical Name: 2-phenyl-1-isobutylcycloethylimine
• CAS No.: 906425-93-2
• Molecular Formula: C₁₂H₁₇N
• Molecular Weight: 175.274
• Mol file: 906425-93-2.mol

Synonyms:2-phenyl-1-isobutylcycloethylimine

Chemical Property of 2-phenyl-1-isobutylcycloethylimine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-phenyl-1-isobutylcycloethylimine

There total 4 articles about 2-phenyl-1-isobutylcycloethylimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

isobutylamine (78-81-9) + (2-bromo-1-phenylethyl)dimethylsulphonium bromide (75326-15-7) → 2-phenyl-1-isobutylcycloethylimine (906425-93-2)

Guidance literature:

In water;

DOI:10.1021/jo800269v

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + isobutylamine (78-81-9) → 2-phenyl-1-isobutylcycloethylimine (906425-93-2)

Guidance literature:

styrene; With dimethylbromosulphonium bromide; In acetonitrile; for 0.166667h; Cooling with ice;

isobutylamine; In water; at 20 ℃;

DOI:10.1039/c1gc15581d

Reference yield:

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) → 2-phenyl-1-isobutylcycloethylimine (906425-93-2)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / 0.17 h / Cooling with ice

2: water / 20 °C

In water; acetonitrile;

DOI:10.1080/00397911.2010.521903

upstream raw materials:

isobutylamine

(2-bromo-1-phenylethyl)dimethylsulphonium bromide

styrene

dimethylbromosulphonium bromide

Downstream raw materials:

3-isobutyl-4-phenyloxazolidin-2-one

3-isobutyl-5-phenyloxazolidin-2-one