benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine

Base Information

Chemical Name:benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine
CAS No.:499142-82-4
Molecular Formula:C₅₅H₇₀NO₈P
Molecular Weight:904.136
Hs Code.:

Synonyms:benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine

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Chemical Property of benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine

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Technology Process of benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine

There total 4 articles about benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 108549-21-9
benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

: 499142-71-1
3,4,5,6-tetra-O-benzyl-2-O-octanoyl-D-myo-inositol

: 499142-82-4
benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine

Guidance literature:: With N,N-diisopropylamine tetrazolide; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1021/ol0202161

Reference yield:

: 24558-77-8
3,4,5,6-tetra-O-benzyl inositol

: 499142-82-4
benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine

Guidance literature:: Multi-step reaction with 4 steps

1.1: dibutyltin oxide / 3 h

1.2: 96 percent / cesium fluoride / toluene; dimethylformamide / -10 - 20 °C

2.1: pyridine / 0 - 20 °C

3.1: 48 percent / palladium(II) chloride; sodium acetate / H₂O; acetic acid / 20 °C

4.1: 93 percent / N,N-diisopropylammonium tetrazolide / CH₂Cl₂ / 5 h / 20 °C

With N,N-diisopropylamine tetrazolide; sodium acetate; di(n-butyl)tin oxide; palladium dichloride; In pyridine; dichloromethane; water; acetic acid;
DOI:10.1021/ol0202161

Reference yield:

: 64681-28-3
D-1-O-allyl-3,4,5,6-tetra-O-benzyl-myo-inositol

: 499142-82-4
benzyloxy-[2-O-octanoyl-3,4,5,6-tetra-O-benzyl-D-myo-inosityl]-(N,N-diisopropylamino)phosphine

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 - 20 °C

2: 48 percent / palladium(II) chloride; sodium acetate / H₂O; acetic acid / 20 °C

3: 93 percent / N,N-diisopropylammonium tetrazolide / CH₂Cl₂ / 5 h / 20 °C

With N,N-diisopropylamine tetrazolide; sodium acetate; palladium dichloride; In pyridine; dichloromethane; water; acetic acid;
DOI:10.1021/ol0202161