C₅₆H₈₃ClNO₁₁P

Base Information

Chemical Name:C₅₆H₈₃ClNO₁₁P
CAS No.:1422356-81-7
Molecular Formula:C₅₆H₈₃ClNO₁₁P
Molecular Weight:1012.7
Hs Code.:

C<sub>56</sub>H<sub>83</sub>ClNO<sub>11</sub>P

Synonyms:C₅₆H₈₃ClNO₁₁P

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Chemical Property of C₅₆H₈₃ClNO₁₁P

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Technology Process of C₅₆H₈₃ClNO₁₁P

There total 23 articles about C₅₆H₈₃ClNO₁₁P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1422355-61-0
(1R,2R,5R,10S,13R,14R,17S,19R)-5-({[1-(4-chlorophenyl)cyclopropyl]carbamoyl}(oxo)methyl)-1,2,14,18,18-pentamethyl-7-oxo-8-(propan-2-yl)pentacyclo[11,8.0.0^2,10.0^5,9.0^14,19]henicos-8-en-17-yl 1-(2-hydroxyethyl)2,2-dimethylbutanedioate

: 137348-86-8
di-tert-butyl diisopropylphosphoramide

: 1422356-81-7
C₅₆H₈₃ClNO₁₁P

Guidance literature:: (1R,2R,5R,10S,13R,14R,17S,19R)-5-({[1-(4-chlorophenyl)cyclopropyl]carbamoyl}(oxo)methyl)-1,2,14,18,18-pentamethyl-7-oxo-8-(propan-2-yl)pentacyclo[11,8.0.0^2,10.0^5,9.0^14,19]henicos-8-en-17-yl 1-(2-hydroxyethyl)2,2-dimethylbutanedioate; di-tert-butyl diisopropylphosphoramide; With 1H-tetrazole; dmap; In dichloromethane; at 20 ℃; for 2h;

With dihydrogen peroxide; In dichloromethane; water; at 0 ℃; for 0.5h;

Reference yield:

: 226384-14-1
(3aR,5aR,5bR,7aR,9S,11aR,11bR,13aS)-3a-(hydroxymethyl)-1-isopropyl-5a,5b,8, 8,11a-pentamethyl-2-oxo-3,3a,4,5,5a,5b,6,7,7a,8,9,10,11,11a,11b,12,13,13a-octadecahydro-2H-cyclopenta[a]chrysen-9-yl acetate

: 1422356-81-7
C₅₆H₈₃ClNO₁₁P

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

2.1: triethylamine / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

4.1: acetic acid; sodium nitrite / dimethyl sulfoxide / 0 - 20 °C

5.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

6.1: hydrogenchloride; water / 20 - 45 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C

8.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

9.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

10.1: dmap; 1H-tetrazole / dichloromethane / 2 h / 20 °C

10.2: 0.5 h / 0 °C

With 1H-tetrazole; hydrogenchloride; dmap; water; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; pyridinium chlorochromate; trifluoroacetic acid; sodium nitrite; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 473-98-3
betulin

: 1422356-81-7
C₅₆H₈₃ClNO₁₁P

Guidance literature:: Multi-step reaction with 14 steps

1.1: triethylamine; dmap / dichloromethane / Reflux

2.1: hydrogen bromide; acetic acid; acetic anhydride / toluene / 1.5 h / 105 °C

3.1: acetic acid; sodium acetate; sodium dichromate dihydrate; acetic anhydride / toluene / 60 °C

4.1: potassium hydroxide / toluene; ethanol / 1 h / 20 °C

5.1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C

6.1: triethylamine / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 2 h / 20 °C

8.1: acetic acid; sodium nitrite / dimethyl sulfoxide / 0 - 20 °C

9.1: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

10.1: hydrogenchloride; water / 20 - 45 °C

11.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 1 h / 20 °C

12.1: trifluoroacetic acid / dichloromethane / 2 h / 20 °C

13.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 20 °C

14.1: dmap; 1H-tetrazole / dichloromethane / 2 h / 20 °C

14.2: 0.5 h / 0 °C

With 1H-tetrazole; hydrogenchloride; dmap; sodium dichromate dihydrate; water; hydrogen bromide; sodium acetate; acetic anhydride; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; pyridinium chlorochromate; trifluoroacetic acid; potassium hydroxide; sodium nitrite; In ethanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;