(E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide

Base Information

Chemical Name:(E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide
CAS No.:1325724-94-4
Molecular Formula:C₁₅H₁₂N₆O
Molecular Weight:292.3
Hs Code.:

Synonyms:(E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide

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Chemical Property of (E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide

Chemical Property:

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Technology Process of (E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide

There total 5 articles about (E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34296-51-0
1-phenyl-1,2,3-triazole-4-carbaldehyde

: 855153-66-1
isoniazid hydrogen chloride

: 1325724-94-4
(E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide

Guidance literature:: With sulfuric acid; In ethanol; at 20 ℃; for 24h;
DOI:10.1016/j.ejmech.2013.12.039

Reference yield:

: 103755-58-4
(1-phenyl-1H-1,2,3-triazole-4-yl)methanol

: 1325724-94-4
(E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C

2: water / 20 °C

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In water; dimethyl sulfoxide;
DOI:10.1021/jm2003624

Reference yield:

: 62-53-3
aniline

: 1325724-94-4
(E)-N'-[(1-phenyl-1H-1,2,3-triazole-4-yl)methylene]isonicotinoylhydrazide

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 - 5 °C

1.2: 0 - 20 °C

2.1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 20 °C / Darkness

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C

4.1: water / 20 °C

With hydrogenchloride; copper(ll) sulfate pentahydrate; sodium L-ascorbate; sodium nitrite; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In water; dimethyl sulfoxide; tert-butyl alcohol; 2.1: Huisgen cycloaddition;
DOI:10.1021/jm2003624