(1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine

Base Information

Chemical Name:(1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine
CAS No.:191480-76-9
Molecular Formula:C₂₉H₃₅NO₂Si
Molecular Weight:457.688
Hs Code.:

Synonyms:(1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine

Chemical Property:

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Technology Process of (1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine

There total 5 articles about (1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 191480-74-7
((1S,4S)-4-Azido-2-benzyloxymethyl-cyclopent-2-enyloxy)-tert-butyl-diphenyl-silane

: 191480-76-9
(1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine

Guidance literature:: With triphenylphosphine; In tetrahydrofuran; water; for 4h; Heating;
DOI:10.1021/jo962124t

Reference yield:

: 110567-21-0
(1S,2R)-2-(benzyloxymethyl)-1-hydroxy-3-cyclopentene

: 191480-76-9
(1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / imidazole / dimethylformamide / 14 h / Ambient temperature

2: 87 percent / sodium azide / dimethylsulfoxide / Ambient temperature

3: 76 percent / sodium metaperiodate / methanol; H₂O / 36 h / Ambient temperature

4: 90 percent / triphenylphosphine / tetrahydrofuran; H₂O / 4 h / Heating

With 1H-imidazole; sodium periodate; sodium azide; triphenylphosphine; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo962124t

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 191480-76-9
(1S,4S)-3-Benzyloxymethyl-4-(tert-butyl-diphenyl-silanyloxy)-cyclopent-2-enylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / imidazole / dimethylformamide / 14 h / Ambient temperature

2: 87 percent / sodium azide / dimethylsulfoxide / Ambient temperature

3: 76 percent / sodium metaperiodate / methanol; H₂O / 36 h / Ambient temperature

4: 90 percent / triphenylphosphine / tetrahydrofuran; H₂O / 4 h / Heating

With 1H-imidazole; sodium periodate; sodium azide; triphenylphosphine; In tetrahydrofuran; methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/jo962124t