(E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Base Information

• Chemical Name: (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester
• CAS No.: 178230-34-7
• Molecular Formula: C₄₃H₆₈O₄
• Molecular Weight: 649.011

Synonyms:(E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Chemical Property of (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

There total 1 articles about (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

cholesterol (57-88-5) + (E)-3-Chlorocarbonyl-acrylic acid bicyclohexyl-4-yl ester → (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (178230-34-7)

Guidance literature:

With sodium; In 1,4-dioxane; at 80 ℃; for 10h;

DOI:10.1021/ja960282w

Reference yield:

2,6-dibutoxyanthracene (134277-70-6) + (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (178230-34-7) → C65H94O6

Guidance literature:

With cholesteryl β-phenylpropionate; cholesterol 2,4-dichlorobenzoate; In 1,3,5-trimethyl-benzene; at 130 ℃; for 48h; Yield given;

DOI:10.1021/ja960282w

Reference yield:

2,6-dibutoxyanthracene (134277-70-6) + (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester (178230-34-7) → C65H94O6 + C65H94O6

Guidance literature:

With cholesteryl β-phenylpropionate; cholesterol 2,4-dichlorobenzoate; In 1,3,5-trimethyl-benzene; at 130 ℃; for 48h; Yield given. Yields of byproduct given;

DOI:10.1021/ja960282w

upstream raw materials:

cholesterol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 178230-34-7 (E)-But-2-enedioic acid bicyclohexyl-4-yl ester (3S,8S,9S,10R,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-2,3,4,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-3-yl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send