2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

Base Information

Chemical Name:2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide
CAS No.:181702-34-1
Molecular Formula:C₁₆H₁₇N₅OS₂
Molecular Weight:359.476
Hs Code.:

Synonyms:2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

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Chemical Property of 2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

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Technology Process of 2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

There total 1 articles about 2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 6289-02-7
1-phenylpyrazolo<3,4-d>pyrimidine-4,6(5H,7H)-dithione

: 59863-66-0
bromo-N-propylacetamide

: 181702-34-1
2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

Guidance literature:: With pyridine; for 2h; Ambient temperature;
DOI:10.1021/jm960052s

Reference yield: 69.0%

: 181702-34-1
2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

: 74-88-4
methyl iodide

: 181702-37-4
2-(4-Methylsulfanyl-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

Guidance literature:: With sodium hydroxide; for 1h; Ambient temperature;
DOI:10.1021/jm960052s

Reference yield:

: 181702-34-1
2-(4-Mercapto-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

: 2-(4-Amino-1-phenyl-1H-pyrazolo[3,4-d]pyrimidin-6-ylsulfanyl)-pentanoic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / aq. NaOH / 1 h / Ambient temperature

2: 70 percent / NH₃ / ethanol / 72 h / 110 °C

With sodium hydroxide; ammonia; In ethanol;
DOI:10.1021/jm960052s