(S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate

Base Information

Chemical Name:(S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate
CAS No.:1262899-11-5
Molecular Formula:BF₄*C₂₄H₃₇FeNPS
Molecular Weight:545.256
Hs Code.:

Synonyms:(S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate

Suppliers and Price of (S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate

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Chemical Property of (S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate

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Technology Process of (S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate

There total 1 articles about (S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: 1262899-10-4
(S)-(-)-2-dicyclohexylphosphinothioyl-1-dimethylaminoferrocene

: 1262899-11-5
(S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate

Guidance literature:: In diethyl ether; (Ar); Schlenk technique; soln. of Fe complex in Et2O was treated with acid at 0°C; stirred for 10 min; filtered; washed (ice-cold Et2O); dried (vac.); elem. anal.;
DOI:10.1016/j.jorganchem.2010.08.042

Reference yield: 82.0%

: 1262899-11-5
(S)-(-)-[2-(dicyclohexylphosphinothioyl)ferrocenyl]-1-dimethylammonium tetrafluoroborate

: 1262899-10-4
(S)-(-)-2-dicyclohexylphosphinothioyl-1-dimethylaminoferrocene

Guidance literature:: With NaHCO₃; In diethyl ether; water; Sonication; (Ar); Schlenk technique; suspn. of Fe complex in satd. aq. NaHCO3 and Et2O was sonicated for 1 min or until dissolved; layers septd.; aq. phase extd. (Et2O); ether layer washed (H2O, brine); dried (Mg2SO4); filtered; concd. (vac.); chromd. (silica gel, hexane/EtOAc, 1/1);
DOI:10.1016/j.jorganchem.2010.08.042