C₁₆H₂₂O₆

Base Information

Chemical Name:C₁₆H₂₂O₆
CAS No.:1446821-31-3
Molecular Formula:C₁₆H₂₂O₆
Molecular Weight:310.347
Hs Code.:

C<sub>16</sub>H<sub>22</sub>O<sub>6</sub>

Synonyms:C₁₆H₂₂O₆

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Chemical Property of C₁₆H₂₂O₆

Chemical Property:

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Technology Process of C₁₆H₂₂O₆

There total 6 articles about C₁₆H₂₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1446821-29-9
C₁₆H₂₀O₆

: 1446821-31-3
C₁₆H₂₂O₆

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; at 20 ℃; for 12h; under 760.051 Torr;
DOI:10.1016/j.tetlet.2013.05.068

Reference yield:

: 64584-92-5
(R)-pent-4-en-2-ol

: 1446821-31-3
C₁₆H₂₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / dichloromethane / 6 h / 20 °C

2: palladium diacetate; potassium phosphate; tris-(o-tolyl)phosphine / tetrahydrofuran; water / 24 h / 20 °C

3: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h

4: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 0 - 20 °C

5: hydrogen; palladium 10% on activated carbon / ethyl acetate / 12 h / 20 °C / 760.05 Torr

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; potassium phosphate; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.tetlet.2013.05.068

Reference yield:

: 1446821-23-3
(2R)-pent-4-en-2-yl 2-bromoacetate

: 1446821-31-3
C₁₆H₂₂O₆

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate; potassium phosphate; tris-(o-tolyl)phosphine / tetrahydrofuran; water / 24 h / 20 °C

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 24 h

3: 2,6-dimethylpyridine; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 1 h / 0 - 20 °C

4: hydrogen; palladium 10% on activated carbon / ethyl acetate / 12 h / 20 °C / 760.05 Torr

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,6-dimethylpyridine; potassium phosphate; trimethylsilyl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; dichloromethane; water; ethyl acetate;
DOI:10.1016/j.tetlet.2013.05.068