C₅₆H₄₆N₂O₂S

Base Information

Chemical Name:C₅₆H₄₆N₂O₂S
CAS No.:1442686-90-9
Molecular Formula:C₅₆H₄₆N₂O₂S
Molecular Weight:811.059
Hs Code.:

C<sub>56</sub>H<sub>46</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C₅₆H₄₆N₂O₂S

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Chemical Property of C₅₆H₄₆N₂O₂S

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Technology Process of C₅₆H₄₆N₂O₂S

There total 6 articles about C₅₆H₄₆N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1442686-89-6
C₅₅H₄₈N₂O₂

: 1442686-90-9
C₅₆H₄₆N₂O₂S

Guidance literature:: In pyridine; at 60 ℃; for 7h; Inert atmosphere;
DOI:10.1021/ol401306h

Reference yield:

: 77-76-9
2,2-dimethoxy-propane

: 1442686-90-9
C₅₆H₄₆N₂O₂S

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene-4-sulfonic acid / benzene / 8 h / Reflux; Inert atmosphere; Dean-Stark

2.1: magnesium / tetrahydrofuran / Cooling with ice; Inert atmosphere

3.1: thionyl chloride; triethylamine / dichloromethane / 3 h / Reflux; Inert atmosphere

3.2: 72 h / 80 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

5.1: pyridine / 7 h / 60 °C / Inert atmosphere

With lithium aluminium tetrahydride; thionyl chloride; toluene-4-sulfonic acid; magnesium; triethylamine; In tetrahydrofuran; pyridine; dichloromethane; benzene;
DOI:10.1021/ol401306h

Reference yield:

: 1442686-88-5
C₅₅H₄₄N₆O₂

: 1442686-90-9
C₅₆H₄₆N₂O₂S

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 0 °C / Inert atmosphere

2: pyridine / 7 h / 60 °C / Inert atmosphere

With lithium aluminium tetrahydride; In tetrahydrofuran; pyridine;
DOI:10.1021/ol401306h