Im-F₈bp-Im

Base Information

Chemical Name:Im-F₈bp-Im
CAS No.:321725-00-2
Molecular Formula:C₁₈H₆F₈N₄
Molecular Weight:430.26
Hs Code.:

Synonyms:Im-F₈bp-Im

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Im-F₈bp-Im

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Technology Process of Im-F₈bp-Im

There total 1 articles about Im-F₈bp-Im which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 288-32-4
1H-imidazole

: 434-90-2
decafluorobiphenyl

: 321724-99-6
Im-F₉bp

: 321725-00-2
Im-F₈bp-Im

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 30 ℃; for 12h;
DOI:10.1021/ja0543088

Reference yield: 17.3%

: 321725-00-2
Im-F₈bp-Im

: 944767-61-7
[(4,7-dimethyl-1,10-phenanthroline)Re(CO)3(THF)][BF₄]

: [(4,7-dimethyl-1,10-phenanthroline)Re(CO)3(NC₃H₃NC₆F₄C₆F₄N₂C₃H₃)][BF₄]

Guidance literature:: In tetrahydrofuran; dichloromethane; Re complex dissolved in CH2Cl2-THF; added to ligand; stirred at 30°C for 2-5 d (monitored by mass spectra); removed from heating; extd. into CH2Cl2; washed with H2O; org. soln. dried (MgSO4); rotary evapd. to dryness; dissolved in CH2Cl2; flash chromd. (silica gel, MeOH-CH2Cl2 3:97 to 40-60); rotary evapd. to dryness;
DOI:10.1021/ja0543088