<2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide

Base Information

Chemical Name:<2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide
CAS No.:76621-71-1
Molecular Formula:C₄₀H₃₁Cl₂NOPS₂*I
Molecular Weight:834.609
Hs Code.:

Synonyms:<2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide

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Chemical Property of <2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide

Chemical Property:

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Technology Process of <2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide

There total 6 articles about <2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 76621-69-7
1-(N-benzoyl-N-methylamino)-2,2-dichloroethenyltriphenylphosphonium iodide

: 106-54-7
p-Chlorothiophenol

: 76621-71-1
<2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide

Guidance literature:: With triethylamine; In methanol; at 20 - 25 ℃; for 48h;

Reference yield: 88.0%

: 76621-56-2
C₃₉H₂₈Cl₂NOPS₂

: 74-88-4
methyl iodide

: 76621-71-1
<2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide

Guidance literature:: With triethylamine; 1) reflux, 10-15 min, 2) 20-25 deg C, 15-20 h;

Reference yield:

: 68490-32-4
N-<2,2-dichloro-1-(triphenylphosphonio)vinyl>benzimidate

: 76621-71-1
<2,2-bis(p-chlorophenylthio)-1-(N-methylbenzamido)vinyl>triphenylphosphonium iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / triethylamine / methanol / 4 h / 20 - 25 °C

2: 92 percent / sodium methoxide / methanol / 24 h / 20 - 25 °C

3: 88 percent / triethylamine / 1) reflux, 10-15 min, 2) 20-25 deg C, 15-20 h

With sodium methylate; triethylamine; In methanol;