L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol

Base Information

• Chemical Name: L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol
• CAS No.: 139765-17-6
• Molecular Formula: C₂₃H₂₆F₂O₅
• Molecular Weight: 420.453

Synonyms:L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol

Chemical Property of L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol

Chemical Property:

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Technology Process of L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol

There total 10 articles about L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

L-3,6-di-O-benzyl-1-O-<(S)-(-)-camphanyl>-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol (139765-18-7,139894-59-0) → L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol (139765-17-6)

Guidance literature:

With sodium hydroxide; In methanol; Heating;

Reference yield: 97.0%

D-3,6-di-O-benzyl-1-O-<(S)-(-)-camphanyl>-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol (139765-18-7,139894-59-0) → D-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol (139765-17-6)

Guidance literature:

With sodium hydroxide; In methanol; for 1h; Heating;

Reference yield: 75.0%

(+/-)-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-myo-inositol (127414-71-5,139894-55-6,139894-57-8) + 2,2-dimethoxy-propane (77-76-9) → (+/-)-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol (139765-17-6)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; for 2h; Ambient temperature;

upstream raw materials:

D-3,6-di-O-benzyl-1-O-<(S)-(-)-camphanyl>-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol

(+/-)-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-myo-inositol

(+/-)-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-1-O--myo-inositol

L-3,6-di-O-benzyl-1-O-<(S)-(-)-camphanyl>-2-deoxy-2,2-difluoro-4,5-O-isopropylidene-myo-inositol

Downstream raw materials:

D-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-myo-inositol

D-2-deoxy-2,2-difluoro-myo-inositol 1,4,5-trisphosphate

L-3,6-di-O-benzyl-2-deoxy-2,2-difluoro-myo-inositol

L-2-deoxy-2,2-difluoro-myo-inositol 1,4,5-trisphosphate

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