4-FLUOROBENZYLMAGNESIUM CHLORIDE 0.25M&

Base Information

• Chemical Name: 4-FLUOROBENZYLMAGNESIUM CHLORIDE 0.25M&
• CAS No.: 38046-82-1
• Molecular Formula: C11H9BrMgO
• Molecular Weight: 261.401
• Hs Code.: 29310099
• Mol file: 38046-82-1.mol

Synonyms:6-Methoxy-2-naphthylmagnesium bromide solution;

Chemical Property of 4-FLUOROBENZYLMAGNESIUM CHLORIDE 0.25M&

Chemical Property:

• Vapor Pressure: 0.0104mmHg at 25°C
• Boiling Point: 35 °C
• Flash Point: -13 °F
• PSA: 9.23000
• Density: 0.966 g/mL at 25 °C
• LogP: 3.49420
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

6-Methoxy-2-naphthylmagnesium bromide solution 0.5 M in THF ^*data from reagent suppliers

Safty Information:

• Pictogram(s): F+;C;F
• Hazard Codes: F+,C,F,Xn
• Statements: 12-14-19-22-34-67-11-40-36/37
• Safety Statements: 9-16-29-33-45-36/37-26

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 4-FLUOROBENZYLMAGNESIUM CHLORIDE 0.25M&

There total 3 articles about 4-FLUOROBENZYLMAGNESIUM CHLORIDE 0.25M& which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Bromo-6-methoxynaphthalene (5111-65-9) → 6-methoxynaphthalen-2-ylmagnesium bromide (38046-82-1)

Guidance literature:

With magnesium; In tetrahydrofuran; at 50 ℃; for 1.33333h;

Reference yield:

(-)-N-methoxy-N-methyl-2-(ethoxycarbonylamino)propionamide → 6-methoxynaphthalen-2-ylmagnesium bromide (38046-82-1)

Guidance literature:

In tetrahydrofuran;

Reference yield:

→ 6-methoxynaphthalen-2-ylmagnesium bromide (38046-82-1)

Guidance literature:

upstream raw materials:

2-Bromo-6-methoxynaphthalene

Downstream raw materials:

6-methoxy-2-propionylnaphthalene

(R,E)-2-methoxy-6-(4-phenylbut-3-en-2-yl)naphthalene

(S)-(-)-1-phenyl-3-(6-methoxy-2-naphthyl)-1-butene

Refernces

• 1、 -. "NAPHTHYLENE DERIVATIVES AS CYTOCHROME P450 INHIBITORS". Page/Page column 109. . Retrieved 2010/02/10.