(E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate

Base Information

• Chemical Name: (E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate
• CAS No.: 1314035-52-3
• Molecular Formula: C₃₀H₃₉NO₁₃
• Molecular Weight: 621.639
• Mol file: 1314035-52-3.mol

Synonyms:(E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate

Chemical Property of (E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate

There total 1 articles about (E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(E)-methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate (1314035-55-6) + acetic anhydride (108-24-7) → (E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate (1314035-52-3)

Guidance literature:

With pyridine; at 20 ℃;

DOI:10.1039/c0ob01176b

Reference yield: 100.0%

(E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate (1314035-52-3) → (E)-methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate (1314035-55-6)

Guidance literature:

With methanol; sodium methylate; at 20 ℃;

DOI:10.1039/c0ob01176b

Reference yield:

(E)-methyl 5-acetamido-4,7,8,9-tetra-O-acetyl-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate (1314035-52-3) → (E)-5-acetamido-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxy-phenyl)-prop-2-enyl)-D-erythro-L-manno-nononic acid (1314035-58-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: methanol; sodium methylate / 20 °C

2.1: sodium hydroxide / water / 20 °C

2.2: Acidic conditions

With methanol; sodium methylate; sodium hydroxide; In water;

DOI:10.1039/c0ob01176b

upstream raw materials:

(E)-methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate

acetic anhydride

Downstream raw materials:

(E)-methyl 5-acetamido-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxyphenyl)-prop-2-enyl)-D-erythro-L-manno-nononate

(E)-5-acetamido-2,6-anhydro-3,5-dideoxy-2-C-(3-(4-methoxy-phenyl)-prop-2-enyl)-D-erythro-L-manno-nononic acid