ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate

Base Information

Chemical Name:ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate
CAS No.:1403655-78-6
Molecular Formula:C₂₃H₂₅NO₆
Molecular Weight:411.455
Hs Code.:

Synonyms:ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate

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Chemical Property of ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate

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Technology Process of ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate

There total 2 articles about ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.5%

: 56999-62-3
ethyl 2-(1-methyl-1H-indol-3-yl)acetate

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 1403655-78-6
ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate

Guidance literature:: ethyl 2-(1-methyl-1H-indol-3-yl)acetate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;

3,4,5-Trimethoxybenzoyl chloride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.2174/157018012802652912

Reference yield:

: 118-41-2
Eudesmic acid

: 1403655-78-6
ethyl 2-(1-methyl-1H-indol-3-yl)-3-(3,4,5-trimethoxyphenyl)-3-oxopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / toluene / Reflux

2.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

2.2: -78 - 20 °C / Inert atmosphere

With thionyl chloride; lithium diisopropyl amide; In tetrahydrofuran; toluene;
DOI:10.2174/157018012802652912