N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide

Base Information

Chemical Name:N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide
CAS No.:1027983-95-4
Molecular Formula:C₂₇H₃₀N₂O₂
Molecular Weight:414.547
Hs Code.:

Synonyms:N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide

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Chemical Property of N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide

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Technology Process of N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide

There total 3 articles about N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 50-47-5
desipramine

: 4693-91-8
4-methoxyphenyl-acetic chloride

: 1027983-95-4
N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide

Guidance literature:: desipramine; With triethylamine; In 1,2-dichloro-ethane; at 20 ℃; for 0.5h;

4-methoxyphenyl-acetic chloride; With triisobutylaluminum; In 1,2-dichloro-ethane; toluene; Reflux;
DOI:10.1016/j.ejmech.2017.09.021

Reference yield:

: 50-49-7
impramine

: 1027983-95-4
N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / 1,2-dichloro-ethane / 1 h / Reflux

2.1: 2 h / Reflux

3.1: triethylamine / 1,2-dichloro-ethane / 0.5 h / 20 °C

3.2: Reflux

With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; triethylamine; In 1,2-dichloro-ethane;
DOI:10.1016/j.ejmech.2017.09.021

Reference yield:

: C₂₀H₂₃ClN₂O₂

: 1027983-95-4
N-[3-(5,6-dihydrobenzo[b][1]benzazepin-11-yl)propyl]-2-(4-methoxyphenyl)-N-methylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2 h / Reflux

2.1: triethylamine / 1,2-dichloro-ethane / 0.5 h / 20 °C

2.2: Reflux

With triethylamine; In 1,2-dichloro-ethane;
DOI:10.1016/j.ejmech.2017.09.021