α-Cyano-β-aminocrotonamide

Base Information

• Chemical Name: α-Cyano-β-aminocrotonamide
• CAS No.: 103607-61-0
• Molecular Formula: C₁₁H₁₀ClN₃O
• Molecular Weight: 235.673

Synonyms:α-Cyano-β-aminocrotonamide

Chemical Property of α-Cyano-β-aminocrotonamide

Chemical Property:

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Technology Process of α-Cyano-β-aminocrotonamide

There total 1 articles about α-Cyano-β-aminocrotonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

α-cyano-β-dimethylaminocrotonamide (62321-92-0) + 4-chloro-aniline (106-47-8) → α-Cyano-β-aminocrotonamide (103607-61-0)

Guidance literature:

In acetic acid; Heating;

DOI:10.1007/BF00767827

Reference yield: 83.0%

α-Cyano-β-aminocrotonamide (103607-61-0) + N,N-dimethylformamide diethyl diacetal (1188-33-6) → α-Cyano-β-(p-chlorophenylamino)(dimethylaminovinyl)acrylic acid N-(dimethylaminomethylene)amide

Guidance literature:

In ethanol; Heating;

DOI:10.1007/BF00767827

Reference yield: 78.0%

α-Cyano-β-aminocrotonamide (103607-61-0) → (1-p-chloroanilinoethylidene)malononitrile (61097-14-1)

Guidance literature:

With trichlorophosphate; In acetonitrile; for 2h; Heating;

DOI:10.1023/A:1017566212124

upstream raw materials:

α-cyano-β-dimethylaminocrotonamide

4-chloro-aniline

Downstream raw materials:

(1-p-chloroanilinoethylidene)malononitrile

2-chloro-4-(4-chloroanilino)pyridine-3-carbonitrile

4-(4-chloroanilino)-2-oxo-1,2-dihydropyridine-3-carbonitrile

4-(4-Chloro-phenylamino)-2-(3-isopropyl-2-phenyl-oxazolidin-5-ylmethoxy)-nicotinonitrile

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