bis(cyclopentadienyl)(butadiene)zirconium

Base Information

Chemical Name:bis(cyclopentadienyl)(butadiene)zirconium
CAS No.:75374-50-4
Molecular Formula:C₁₄H₁₆Zr
Molecular Weight:275.505
Hs Code.:

Synonyms:bis(cyclopentadienyl)(butadiene)zirconium

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Chemical Property of bis(cyclopentadienyl)(butadiene)zirconium

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Technology Process of bis(cyclopentadienyl)(butadiene)zirconium

There total 1 articles about bis(cyclopentadienyl)(butadiene)zirconium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109586-38-1
Cp₂Zr(C₄H₆)(OC)Co(CO)Cp

: 12078-25-0,12078-23-8
dicarbonylcyclopentadienylcobalt

: 75374-50-4
bis(cyclopentadienyl)(butadiene)zirconium

Guidance literature:: In ⁽²⁾H₈-toluene; cryst. educt dissolved in toluene-d8 at ambient temp.; not isolated; detected by NMR;
DOI:10.1021/om00152a022

Reference yield: 92.0%

: 75374-50-4
bis(cyclopentadienyl)(butadiene)zirconium

: 100-47-0
benzonitrile

: 139705-57-0
(C₅H₅)2Zr(NHC(C₆H₅)CHCH(CHCH₂))

Guidance literature:: In toluene; Ar atmosphere; addn. of soln. of org. compd. in toluene to soln. of Zr-compd. in toluene (0°C, within 1.5 h), stirring (3 h, room temp.); filtration, concn. (vac.), pptn. on addn. of pentane, filtration, drying (vac.); elem. anal.;

Reference yield: 91.0%

: 623-26-7
terephthalonitrile

: 75374-50-4
bis(cyclopentadienyl)(butadiene)zirconium

: (2E,5E,8E)-1,1-bis(η-cyclopentadienyl)-3,8-bis(4'-cyanophenyl)-1-zircona-2,9-diazacyclonona-2,5,8-triene

Guidance literature:: In toluene; Ar; equimolar amounts; stirring at room temperature for 3 d;; filtration; washing of the product with toluene; drying in vacuo; elem. anal.;;
DOI:10.1021/om00029a055