2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine

Base Information

• Chemical Name: 2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine
• CAS No.: 548492-22-4
• Molecular Formula: C₂₅H₄₄N₂
• Molecular Weight: 372.638
• Mol file: 548492-22-4.mol

Synonyms:2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine

Chemical Property of 2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine

There total 2 articles about 2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2,3-butanedione (2,6-diisopropylphenyl)(n-octyl)bis-imine + trimethylaluminum (75-24-1) → 2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine (548492-22-4) + C25H44N2 (548492-29-1)

Guidance literature:

2,3-butanedione (2,6-diisopropylphenyl)(n-octyl)bis-imine; trimethylaluminum; In toluene; at 0 - 20 ℃; for 144h;

With sodium hydroxide; water; In toluene;

Reference yield:

1,4-bis(2,6-diisopropylphenyl)-2,3-dimethyl-1,4-diazabuta-1,3-diene → 2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine (548492-22-4)

Guidance literature:

Multi-step reaction with 3 steps

1: toluene / 21 h / 60 °C / Inert atmosphere

2: sulfuric acid / ethanol; water / 3 - 4.5 h / 40 - 65 °C / Inert atmosphere

3: formic acid / toluene / Inert atmosphere; Reflux

With formic acid; sulfuric acid; In ethanol; water; toluene;

DOI:10.1021/acs.oprd.5b00047

Reference yield: 86.9%

2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine (548492-22-4) + methylmagnesium bromide (75-16-1) + hafnium tetrachloride (13499-05-3) → (N-(1,1-dimethyl-2-(octylimino-κN)-propyl )-2,6-d i isopropylbenzenaminato-κN)-trimethylhafnium

Guidance literature:

2,6-diisopropyl-N-(2-methyl-3-(octyliminobutan-2-yl))benzenamine; hafnium tetrachloride; In toluene; at 23 ℃; for 0.5h; Inert atmosphere;

methylmagnesium bromide; In diethyl ether; toluene; at 0 - 23 ℃; Inert atmosphere;

DOI:10.1021/acs.oprd.5b00047

upstream raw materials:

trimethylaluminum