N-methyl>methyl>-N^α-(benzyloxycarbonyl)glycinamide

Base Information

• Chemical Name: N-methyl>methyl>-N^α-(benzyloxycarbonyl)glycinamide
• CAS No.: 91202-75-4
• Molecular Formula: C₅₆H₇₄N₂O₃₃
• Molecular Weight: 1303.2

Synonyms:N-methyl>methyl>-N^α-(benzyloxycarbonyl)glycinamide

Chemical Property of N-methyl>methyl>-N^α-(benzyloxycarbonyl)glycinamide

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Technology Process of N-methyl>methyl>-N^α-(benzyloxycarbonyl)glycinamide

There total 5 articles about N-methyl>methyl>-N^α-(benzyloxycarbonyl)glycinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1-bromo-2,3,4,6-tetra-O-acetyl-D-galactopyranose (3068-32-4) + N-<2-hydroxy-1,1-bis(hydroxymethyl)ethyl>-Nα-(benzyloxycarbonyl)glycinamide (91202-74-3) → N-methyl>methyl>-Nα-(benzyloxycarbonyl)glycinamide (91202-75-4)

Guidance literature:

With mercury(II) cyanide; In acetonitrile; Ambient temperature;

DOI:10.1016/0009-3084(95)02475-X

Reference yield: 65.0%

N-<2-hydroxy-1,1-bis(hydroxymethyl)ethyl>-Nα-(benzyloxycarbonyl)glycinamide (91202-74-3) + 1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside (3068-32-4) → N-methyl>methyl>-Nα-(benzyloxycarbonyl)glycinamide (91202-75-4)

Guidance literature:

With mercury(II) cyanide; In acetonitrile; ultrasonication;

DOI:10.1016/S0040-4039(00)76654-8

Reference yield: 23.7%

2-(acetoxymethyl)-6-bromotetrahydro-2H-pyran-3,4,5-triyl triacetate (529493-92-3) + N-<2-hydroxy-1,1-bis(hydroxymethyl)ethyl>-Nα-(benzyloxycarbonyl)glycinamide (91202-74-3) → N-methyl>methyl>-Nα-(benzyloxycarbonyl)glycinamide (91202-75-4)

Guidance literature:

With mercury(II) cyanide; mercury dibromide; In acetonitrile; Ambient temperature;

DOI:10.1021/jm00376a014

upstream raw materials:

1-bromo-2,3,4,6-tetra-O-acetyl-D-galactopyranose

N-<2-hydroxy-1,1-bis(hydroxymethyl)ethyl>-N^α-(benzyloxycarbonyl)glycinamide

2-(acetoxymethyl)-6-bromotetrahydro-2H-pyran-3,4,5-triyl triacetate

1-bromo-1-deoxy-2,3,4,6-tetra-O-acetyl-a-D-galactopyranoside

Downstream raw materials:

N^α-benzyloxycarbonyl-N-[tris(β-D-galactopyranosyloxymethyl)methyl]glycinamide

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