(S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide

Base Information

Chemical Name:(S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide
CAS No.:449728-87-4
Molecular Formula:C₃₂H₃₉N₃O₄
Molecular Weight:529.679
Hs Code.:

Synonyms:(S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide

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Chemical Property of (S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide

Chemical Property:

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Technology Process of (S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide

There total 5 articles about (S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3946-32-5
suberic acid monomethyl ester

: 449728-87-4
(S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

2: 68 percent / aq. LiOH / tetrahydrofuran / 20 °C

3: NMM / tetrahydrofuran

4: 420 mg / NMM / tetrahydrofuran / 2.25 h

With 4-methyl-morpholine; lithium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0208119

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 449728-87-4
(S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / iPr₂NEt; BOP-Cl / CH₂Cl₂

2: 68 percent / aq. LiOH / tetrahydrofuran / 20 °C

3: NMM / tetrahydrofuran

4: 420 mg / NMM / tetrahydrofuran / 2.25 h

With 4-methyl-morpholine; lithium hydroxide; bis-(2-oxo-3-oxazolidinyl)phosphoryl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm0208119

Reference yield:

: 251304-81-1
8-((benzyloxy)amino)-8-oxooctanoic acid

: 449728-87-4
(S)-octanedioic acid benzyloxy-amide (1-phenethylcarbamoyl-2-phenyl-ethyl)amide

Guidance literature:: Multi-step reaction with 2 steps

1: NMM / tetrahydrofuran

2: 420 mg / NMM / tetrahydrofuran / 2.25 h

With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1021/jm0208119