(8R)-8-benzyloxynonan-1-ol

Base Information

Chemical Name:(8R)-8-benzyloxynonan-1-ol
CAS No.:202405-19-4
Molecular Formula:C₁₆H₂₆O₂
Molecular Weight:250.381
Hs Code.:

Synonyms:(8R)-8-benzyloxynonan-1-ol

Suppliers and Price of (8R)-8-benzyloxynonan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (8R)-8-benzyloxynonan-1-ol

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Technology Process of (8R)-8-benzyloxynonan-1-ol

There total 8 articles about (8R)-8-benzyloxynonan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 202405-18-3
((R)-8-Benzyloxy-nonyloxy)-tert-butyl-dimethyl-silane

: 202405-19-4
(8R)-8-benzyloxynonan-1-ol

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 ℃;

Reference yield:

: 629-41-4
1,8-Octanediol

: 202405-19-4
(8R)-8-benzyloxynonan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 48 percent / Et₃N, DMAP / CH₂Cl₂ / 6 h

2: 84 percent / PCC, NaOAc / CH₂Cl₂ / 3 h

3: 89 percent / diethyl ether / 3 h / 0 °C

4: porcine pancreatic lipase / diisopropyl ether / 18 h

5: 97 percent / 2N alcoholic KOH / 12 h / Ambient temperature

6: 1.) NaH / 1.) THF, 60 deg C, 1 h, 2.) THF, RT, overnight

7: 88 percent / Bu₄NF / tetrahydrofuran / -78 °C

With dmap; potassium hydroxide; porcine pancreatic lipase; tetrabutyl ammonium fluoride; sodium acetate; sodium hydride; triethylamine; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; dichloromethane; di-isopropyl ether;

Reference yield:

: 128622-13-9
8-(tert-butyl)dimethylsilyloxyoctanal

: 202405-19-4
(8R)-8-benzyloxynonan-1-ol

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / diethyl ether / 3 h / 0 °C

2: porcine pancreatic lipase / diisopropyl ether / 18 h

3: 97 percent / 2N alcoholic KOH / 12 h / Ambient temperature

4: 1.) NaH / 1.) THF, 60 deg C, 1 h, 2.) THF, RT, overnight

5: 88 percent / Bu₄NF / tetrahydrofuran / -78 °C

With potassium hydroxide; porcine pancreatic lipase; tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; diethyl ether; di-isopropyl ether;