diphenyl-α-nitromethylisopropylphosphine oxide

Base Information

• Chemical Name: diphenyl-α-nitromethylisopropylphosphine oxide
• CAS No.: 81200-75-1
• Molecular Formula: C₁₆H₁₈NO₃P
• Molecular Weight: 303.298
• Mol file: 81200-75-1.mol

Synonyms:diphenyl-α-nitromethylisopropylphosphine oxide

Chemical Property of diphenyl-α-nitromethylisopropylphosphine oxide

Chemical Property:

Purity/Quality:

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Technology Process of diphenyl-α-nitromethylisopropylphosphine oxide

There total 1 articles about diphenyl-α-nitromethylisopropylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

5-methoxy-4,4-dimethyl-5,5-diphenyl-Δ2-1,2,5λ5-oxazaphospholine 2-oxide (81200-74-0) → diphenyl-α-nitromethylisopropylphosphine oxide (81200-75-1)

Guidance literature:

With water; In 1,4-dioxane; at 50 - 55 ℃; for 12h;

Reference yield:

diphenyl-α-nitromethylisopropylphosphine oxide (81200-75-1) → 1-Nitro-2-methyl-1-propen (1606-30-0) + diphenylphosphinous acid methyl ester (4020-99-9)

Guidance literature:

at 170 ℃;

upstream raw materials:

5-methoxy-4,4-dimethyl-5,5-diphenyl-Δ²-1,2,5λ⁵-oxazaphospholine 2-oxide

Downstream raw materials:

1-Nitro-2-methyl-1-propen

diphenylphosphinous acid methyl ester