Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester

Base Information

Chemical Name:Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester
CAS No.:498554-93-1
Molecular Formula:C₆₀H₈₉O₁₀P
Molecular Weight:1001.33
Hs Code.:

Synonyms:Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester

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Chemical Property of Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester

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Technology Process of Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester

There total 7 articles about Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108549-21-9
benzyl-N,N,N',N'-tetraisopropylphosphorodiamidite

: 498554-93-1
Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / diisopropylammonium tetrazolide / CH₂Cl₂ / 1 h / 20 °C

2: 1H-tetrazole / CH₂Cl₂ / 20 °C

3: 89 mg / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0 - 20 °C

With 1H-tetrazole; N,N-diisopropylamine tetrazolide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja0285159

Reference yield:

: 83167-59-3
1-O-octadecyl-2-O-methyl-sn-glycerol

: 498554-93-1
Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / diisopropylammonium tetrazolide / CH₂Cl₂ / 1 h / 20 °C

2: 1H-tetrazole / CH₂Cl₂ / 20 °C

3: 89 mg / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0 - 20 °C

With 1H-tetrazole; N,N-diisopropylamine tetrazolide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/ja0285159

Reference yield:

: 162792-20-3
(1R,2R,3S,4S,5R)-3,4,5-Tris-benzyloxy-cyclohexane-1,2-diol

: 498554-93-1
Phosphoric acid benzyl ester (R)-2-methoxy-3-octadecyloxy-propyl ester (1R,2R,3S,4R,6R)-2,3,4-tris-benzyloxy-6-isobutoxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: Bu₂SnO / toluene / 2 h / Heating

1.2: 90 percent / CsF / dimethylformamide / 20 °C

2.1: 17 percent / NaH; Bu₄NI / dimethylformamide / 4 h / 0 °C

3.1: 79 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.33 h / 0 °C

4.1: 1H-tetrazole / CH₂Cl₂ / 20 °C

5.1: 89 mg / m-chloroperoxybenzoic acid / CH₂Cl₂ / 0 - 20 °C

With 1H-tetrazole; ammonium cerium(IV) nitrate; tetra-(n-butyl)ammonium iodide; sodium hydride; di(n-butyl)tin oxide; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ja0285159