2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

Base Information

Chemical Name:2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane
CAS No.:137853-36-2
Molecular Formula:C₃₀H₄₆O₂S₂
Molecular Weight:502.826
Hs Code.:

Synonyms:2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

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Chemical Property of 2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

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Technology Process of 2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

There total 8 articles about 2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 137853-35-1
2-isopropyl-2-(1-benzoxyl-5-phenylsulfonyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

: 137853-36-2
2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

Guidance literature:: With disodium hydrogenphosphate; sodium amalgam; In methanol; for 0.5h; Ambient temperature;
DOI:10.1080/00397919108021291

Reference yield:

: 64418-59-3
3,7-dimethyl-8-chloro-2(E),6(E)-octadien-1-yl acetate

: 137853-36-2
2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 50percent aq. NaOH, TBAB / 5 h / Ambient temperature

2: methanolic K₂CO₃ / 1 h / Ambient temperature

3: 47 percent / 6percent sodium amalgam, NaHPO₄ / methanol / 1 h / 0 °C

With sodium hydroxide; sodium amalgam; camphor-10-sulfonic acid; tetrabutylammomium bromide; potassium carbonate; In methanol;

Reference yield:

: 137853-32-8,137853-33-9,143658-39-3,143658-40-6
syn,anti-2-isopropyl-2-(3-methyl-2-hydroxy-1-benzyloxy-4-pentenyl)-1,3-dithiane

: 137853-36-2
2-isopropyl-2-(1-benzoxyl-13-hydroxyl-3,7,11-trimethyl-3E,7E,11E-tridecatrienyl)-1,3-dithiocyclohexane

Guidance literature:: Multi-step reaction with 5 steps

1: PBr₃, pyridine / light petroleum / 2 h / 0 °C

2: 45 percent / dimethylformamide / 20 h / Ambient temperature

3: 50percent aq. NaOH, TBAB / 5 h / Ambient temperature

4: methanolic K₂CO₃ / 1 h / Ambient temperature

5: 47 percent / 6percent sodium amalgam, NaHPO₄ / methanol / 1 h / 0 °C

With pyridine; sodium hydroxide; sodium amalgam; camphor-10-sulfonic acid; tetrabutylammomium bromide; phosphorus tribromide; potassium carbonate; In methanol; N,N-dimethyl-formamide; Petroleum ether;