(-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate

Base Information

Chemical Name:(-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate
CAS No.:1082074-13-2
Molecular Formula:C₃₃H₄₁NO₇SSi
Molecular Weight:623.843
Hs Code.:

Synonyms:(-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate

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Chemical Property of (-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate

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Technology Process of (-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate

There total 1 articles about (-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 773-64-8
2-mesitylenesulphonyl chloride

: 1082074-12-1
(+)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl hydroxycarbamate

: 1082074-13-2
(-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; toluene; at 0 ℃; for 1h;
DOI:10.1021/jo8015709

Reference yield: 74.0%

: 1082074-13-2
(-)-(3S,6S)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-3,6-dihydro-2H-pyran-3-yl mesitylsulfonyloxycarbamate

: 1082074-14-3
(-)-(3aS,6S,7R,7aS)-6-[2-(tert-butyldiphenylsilyloxy)ethyl]-7-hydroxytetrahydro-1H-pyrano[4,3-d]oxazol-2(6H)-one

Guidance literature:: With potassium osmate(VI) dihydrate; N-ethyl-N,N-diisopropylamine; In propan-1-ol; water; at 20 ℃; for 5h;
DOI:10.1021/jo8015709