tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

Base Information

Chemical Name:tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate
CAS No.:173265-29-7
Molecular Formula:C₃₈H₅₁F₃O₈
Molecular Weight:692.813
Hs Code.:

Synonyms:tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

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Technology Process of tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

There total 1 articles about tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 619-21-6
m-formylphenyl benzoic acid

: 130781-88-3
tert-butyl 3α,7α-dihydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

: 173265-29-7
tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; Ambient temperature;

Reference yield: 80.0%

: 173265-29-7
tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

: 173265-30-0
3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 1.5h;

Reference yield:

: 173265-29-7
tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

: 173265-31-1
Benzyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / TFA / CH₂Cl₂ / 1.5 h

2: 75 percent / DCC, DMAP / 3 h

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane;