3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

Base Information

Chemical Name:3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid
CAS No.:173265-30-0
Molecular Formula:C₃₄H₄₃F₃O₈
Molecular Weight:636.706
Hs Code.:

Synonyms:3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

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Chemical Property of 3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

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Technology Process of 3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

There total 3 articles about 3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 173265-29-7
tert-Butyl 3α-(3-formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

: 173265-30-0
3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 1.5h;

Reference yield:

: 619-21-6
m-formylphenyl benzoic acid

: 173265-30-0
3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / DCC, DMAP / CH₂Cl₂; dimethylformamide / Ambient temperature

2: 80 percent / TFA / CH₂Cl₂ / 1.5 h

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 130781-88-3
tert-butyl 3α,7α-dihydroxy-12α-trifluoroacetoxy-5β-cholan-24-oate

: 173265-30-0
3α-(3-Formylbenzoyloxy)-7α-hydroxy-12α-trifluoroacetoxy-5β-cholan-24-oic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / DCC, DMAP / CH₂Cl₂; dimethylformamide / Ambient temperature

2: 80 percent / TFA / CH₂Cl₂ / 1.5 h

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;