4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol

Base Information

• Chemical Name: 4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol
• CAS No.: 1434821-59-6
• Molecular Formula: C₆₉H₇₂O₁₃
• Molecular Weight: 1109.32

Synonyms:4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol

Chemical Property of 4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol

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Technology Process of 4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol

There total 1 articles about 4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

3-O-(4-bromobenzyl)-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol (1434821-53-0) + 3,4-Dimethoxyphenylboronic acid (122775-35-3) → 4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol (1434821-59-6)

Guidance literature:

With potassium phosphate; tetrabutylammomium bromide; palladium diacetate; In ethanol; at 20 ℃; for 3h; Schlenk technique; Inert atmosphere;

DOI:10.1021/jo4004184

Reference yield: 80.0%

4,5-di-O-benzyl-3-O-(4-(3,4-dimethoxyphenyl)benzyl)-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol (1434821-59-6) + benzyl bromide (100-39-0) → 3-O-(4-(3,4-dimethoxyphenyl)benzyl)-1,2,4,5-tetra-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myoinositol (1434821-65-4)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃;

DOI:10.1021/jo4004184

upstream raw materials:

3-O-(4-bromobenzyl)-4,5-di-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myo-inositol

3,4-Dimethoxyphenylboronic acid

Downstream raw materials:

3-O-(4-(3,4-dimethoxyphenyl)benzyl)-1,2,4,5-tetra-O-benzyl-6-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)-L-myoinositol

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