1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide

Base Information

• Chemical Name: 1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide
• CAS No.: 183056-01-1
• Molecular Formula: C₁₇H₂₀N₃O₂P
• Molecular Weight: 329.338

Synonyms:1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide

Chemical Property of 1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide

Chemical Property:

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Technology Process of 1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide

There total 4 articles about 1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

[1-(2-Chloro-ethyl)-3-(4-methoxy-phenyl)-2-oxo-2λ5-[1,3,2]diazaphospholidin-2-yl]-phenyl-amine (183055-95-0) → 1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide (183056-01-1)

Guidance literature:

With tetrabutylammomium bromide; sodium hydride; In benzene; for 5h; Ambient temperature;

DOI:10.1055/s-1996-4364

Reference yield:

N-bis(2-chloroethyl)-N'-phenylphosphodiamidochloridate (53382-80-2) → 1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide (183056-01-1)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / 96 h / Ambient temperature

2: methanol / 20 h / Ambient temperature

3: 94 percent / NaH, Bu₄NBr / benzene / 5 h / Ambient temperature

With tetrabutylammomium bromide; sodium hydride; triethylamine; In methanol; dichloromethane; benzene;

DOI:10.1055/s-1996-4364

Reference yield:

aniline (62-53-3) → 1-(4-Methoxy-phenyl)-7-phenyl-tetrahydro-[1,3,2]diazaphospholo[1,2-a][1,3,2]diazaphosphole 8-oxide (183056-01-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 64 percent / CH₂Cl₂ / 240 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 96 h / Ambient temperature

3: methanol / 20 h / Ambient temperature

4: 94 percent / NaH, Bu₄NBr / benzene / 5 h / Ambient temperature

With tetrabutylammomium bromide; sodium hydride; triethylamine; In methanol; dichloromethane; benzene;

DOI:10.1055/s-1996-4364

upstream raw materials:

[1-(2-Chloro-ethyl)-3-(4-methoxy-phenyl)-2-oxo-2λ⁵-[1,3,2]diazaphospholidin-2-yl]-phenyl-amine

N-bis(2-chloroethyl)-N'-phenylphosphodiamidochloridate

aniline

N-bis(2-chloroethyl)-N'-(4-methoxyphenyl)-N''-phenylphosphotriamidate

Downstream raw materials:

9-methoxy-1-phenyl-2,3,5,6-tetrahydro-1H,4H-1,3a,6-triaza-10b-phospha-benzo[e]azulene 10b-oxide

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