2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene

Base Information

• Chemical Name: 2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene
• CAS No.: 1384107-34-9
• Molecular Formula: C₁₅H₁₅Cl₄NO₂S
• Molecular Weight: 415.168

Synonyms:2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene

Chemical Property of 2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene

Chemical Property:

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Technology Process of 2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene

There total 1 articles about 2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

pentachloro-2-nitro-1,3-butadiene (61351-34-6) + 4-tert-butylbenzyl mercaptan (49543-63-7) → 2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene (1384107-34-9)

Guidance literature:

at 20 ℃;

DOI:10.1080/10426507.2012.657313

Reference yield: 86.0%

2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene (1384107-34-9) + 1-(4-Fluorophenyl)piperazine (2252-63-3) → 1-[4-(4-fluorophenyl)piperazinyl]-2-nitro-1-[(4-tert-butylbenzyl)thio]-3,4,4-trichloro-1,3-butadiene (1384107-40-7)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1080/10426507.2012.657313

Reference yield: 85.0%

Thiomorpholin (123-90-0) + 2-nitro-1-[(4-tert-butylbenzyl)thio]-1,3,4,4-tetrachloro-1,3-butadiene (1384107-34-9) → 4-(1-thiomorpholinyl)-4-(4-tert-butylbenzylsulfanyl)-1,1,2-trichloro-3-nitro-1,3-butadiene

Guidance literature:

In dichloromethane; at 20 ℃; for 24h;

DOI:10.1080/10426507.2015.1024789

upstream raw materials:

pentachloro-2-nitro-1,3-butadiene

4-tert-butylbenzyl mercaptan

Downstream raw materials:

1-morpholino-2-nitro-1-[(4-tert-butylbenzyl)thio]-3,4,4-trichloro-1,3-butadiene

N,N'-bis[2-nitro-1-[(4-tert-butylbenzyl)thio]-3,4,4-trichloro-1,3-butadienyl]piperazine

1-(4-methylpiperazinyl)-2-nitro-1-[(4-tert-butylbenzyl)thio]-3,4,4-trichloro-1,3-butadiene

1-[4-(4-fluorophenyl)piperazinyl]-2-nitro-1-[(4-tert-butylbenzyl)thio]-3,4,4-trichloro-1,3-butadiene

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