C₂₃H₂₅NO₇

Base Information

Chemical Name:C₂₃H₂₅NO₇
CAS No.:1335287-18-7
Molecular Formula:C₂₃H₂₅NO₇
Molecular Weight:427.454
Hs Code.:

C<sub>23</sub>H<sub>25</sub>NO<sub>7</sub>

Synonyms:C₂₃H₂₅NO₇

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Chemical Property of C₂₃H₂₅NO₇

Chemical Property:

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Technology Process of C₂₃H₂₅NO₇

There total 21 articles about C₂₃H₂₅NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1335287-17-6
C₂₃H₂₉NO₇

: 1335287-18-7
C₂₃H₂₅NO₇

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2011.08.014

Reference yield:

: ethyl (2E,4S,5S)-5-((tert-butyldimethylsilyl)oxy)-4-hydroxy-2-hexenoate

: 1335287-18-7
C₂₃H₂₅NO₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: triphenylphosphine; diethylazodicarboxylate / toluene; benzene / 2 h / 0 - 20 °C / Inert atmosphere

2.1: methanol; ammonia / water / 3 h / 0 - 20 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydroxide / tetrahydrofuran; methanol; water / 2 h / 0 - 20 °C

4.2: pH 3 - 4

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

6.1: water; acetic acid / tetrahydrofuran / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 °C / Inert atmosphere

9.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C / Inert atmosphere

10.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

11.1: Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; methanol; dmap; tetrabutyl ammonium fluoride; ammonia; water; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; water; toluene; benzene; 11.1: Dess-Martin oxidation;
DOI:10.1016/j.tet.2011.08.014

Reference yield:

: 1335286-67-3
N-(tert-butoxycarbonyl)-N-[(1R,2S)-2-tert-butyldiphenylsilyloxy-1-methyl-3-butenyl]amine

: 1335287-18-7
C₂₃H₂₅NO₇

Guidance literature:: Multi-step reaction with 11 steps

1.1: trifluoroacetic acid / dichloromethane / 1 h / 0 °C / Inert atmosphere

1.2: Inert atmosphere; Saturated solution

2.1: 2-picoline borane complex; acetic acid / methanol / 0.5 h / 0 - 20 °C / Inert atmosphere

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 °C / Inert atmosphere

5.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 °C / Inert atmosphere

6.1: water; acetic acid / tetrahydrofuran / Inert atmosphere

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 20 °C / Inert atmosphere

9.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 20 °C / Inert atmosphere

10.1: trifluoroacetic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

11.1: Dess-Martin periodane / dichloromethane / 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; 2-picoline borane complex; tetrabutyl ammonium fluoride; water; Dess-Martin periodane; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 11.1: Dess-Martin oxidation;
DOI:10.1016/j.tet.2011.08.014