Ethanone, 2-chloro-1-(1-methylcyclohexyl)- (9CI)

Base Information

Chemical Name:Ethanone, 2-chloro-1-(1-methylcyclohexyl)- (9CI)
CAS No.:39199-11-6
Molecular Formula:C9H15 Cl O
Molecular Weight:174.671
Hs Code.:
Mol file:39199-11-6.mol

Synonyms:2-Chloro-1-(1-methylcyclohexyl)ethanone

Suppliers and Price of Ethanone, 2-chloro-1-(1-methylcyclohexyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of Ethanone, 2-chloro-1-(1-methylcyclohexyl)- (9CI)

Chemical Property:

Boiling Point:160 °C (12 mmHg)
PSA：17.07000
LogP:2.76470

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethanone, 2-chloro-1-(1-methylcyclohexyl)- (9CI)

There total 3 articles about Ethanone, 2-chloro-1-(1-methylcyclohexyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 83391-73-5
1-chloro-2-(1'-methylcyclohexyl)-2-phenoxyethylene

: 39199-11-6
1-chloro-2-(1-methyl-cyclohexyl)-2-oxoethane

Guidance literature:: With hydrogenchloride; In formic acid;

Reference yield: 65.2%

: 2890-61-1
1-methyl-1-cyclohexancarboxylic acid chloride

: 18107-18-1
diazomethyl-trimethyl-silane

: 39199-11-6
1-chloro-2-(1-methyl-cyclohexyl)-2-oxoethane

Guidance literature:: 1-methyl-1-cyclohexancarboxylic acid chloride; diazomethyl-trimethyl-silane; With triethylamine; In diethyl ether; at -20 - 0 ℃; for 2h;

With hydrogenchloride; In diethyl ether; at -20 - 20 ℃; for 2h;

Reference yield:

: 1123-25-7
1-methyl-1-cyclohexanecarboxylic acid

: 39199-11-6
1-chloro-2-(1-methyl-cyclohexyl)-2-oxoethane

Guidance literature:: Multi-step reaction with 2 steps

1.1: thionyl chloride / dichloromethane / 3 h / 0 - 20 °C

2.1: triethylamine / diethyl ether / 2 h / -20 - 0 °C

2.2: 2 h / -20 - 20 °C

With thionyl chloride; triethylamine; In diethyl ether; dichloromethane;