α-ethenyl-2-formylbenzenemethanol acetate

Base Information

Chemical Name:α-ethenyl-2-formylbenzenemethanol acetate
CAS No.:1206880-31-0
Molecular Formula:C₁₂H₁₂O₃
Molecular Weight:204.225
Hs Code.:

Synonyms:α-ethenyl-2-formylbenzenemethanol acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-ethenyl-2-formylbenzenemethanol acetate

Chemical Property:

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Technology Process of α-ethenyl-2-formylbenzenemethanol acetate

There total 7 articles about α-ethenyl-2-formylbenzenemethanol acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1206880-30-9
α-ethenyl-2-(diethoxymethyl)benzenemethanol acetate

: 1206880-31-0
α-ethenyl-2-formylbenzenemethanol acetate

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 4h;
DOI:10.1021/acs.joc.9b02693

Reference yield: 82.0%

: 1309781-79-0
1-(2-(1,3-dioxolan-2-yl)phenyl)allyl acetate

: 1206880-31-0
α-ethenyl-2-formylbenzenemethanol acetate

Guidance literature:: With hydrogenchloride; In water; ethyl acetate; at 20 ℃;
DOI:10.1002/anie.201008160

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1206880-31-0
α-ethenyl-2-formylbenzenemethanol acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene-4-sulfonic acid / ethanol / 6 h / Reflux

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 1.5 h / -78 - 20 °C / Inert atmosphere

3.1: tetrahydrofuran / 12 h / 0 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: hydrogenchloride / tetrahydrofuran; water / 4 h / 20 °C

With hydrogenchloride; n-butyllithium; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol; hexane; water;
DOI:10.1021/acs.joc.9b02693