2-phenyl-1,2,3,4-d4-quinoxaline

Base Information

Chemical Name:2-phenyl-1,2,3,4-d4-quinoxaline
CAS No.:1262802-10-7
Molecular Formula:C₁₄H₁₀N₂
Molecular Weight:210.215
Hs Code.:

Synonyms:2-phenyl-1,2,3,4-d4-quinoxaline

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Chemical Property of 2-phenyl-1,2,3,4-d4-quinoxaline

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Technology Process of 2-phenyl-1,2,3,4-d4-quinoxaline

There total 5 articles about 2-phenyl-1,2,3,4-d4-quinoxaline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1262802-09-4
2-(2-iodophenyl-d₄)quinoxaline

: 1262802-10-7
2-phenyl-1,2,3,4-d4-quinoxaline

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; water; at 25 ℃;
DOI:10.1002/chem.201002581

Reference yield:

: 1262802-08-3
2-(phenyl-d₅)quinoxaline

: 1262802-10-7
2-phenyl-1,2,3,4-d4-quinoxaline

Guidance literature:: Multi-step reaction with 2 steps

1: [bis(acetoxy)iodo]benzene; palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid / 8 h / 120 °C

2: ammonium chloride; zinc / tetrahydrofuran; water / 25 °C

With [bis(acetoxy)iodo]benzene; palladium diacetate; tetra-(n-butyl)ammonium iodide; ammonium chloride; acetic acid; zinc; In tetrahydrofuran; water;
DOI:10.1002/chem.201002581

Reference yield:

: 28077-64-7
acetophenone-d5

: 1262802-10-7
2-phenyl-1,2,3,4-d4-quinoxaline

Guidance literature:: Multi-step reaction with 4 steps

1: tetra-N-butylammonium tribromide / methanol; dichloromethane / 2 h / 30 °C

2: ClHO₄*O₂Si / acetonitrile / 20 °C

3: [bis(acetoxy)iodo]benzene; palladium diacetate; tetra-(n-butyl)ammonium iodide; acetic acid / 8 h / 120 °C

4: ammonium chloride; zinc / tetrahydrofuran; water / 25 °C

With [bis(acetoxy)iodo]benzene; ClHO₄*O₂Si; palladium diacetate; tetra-N-butylammonium tribromide; tetra-(n-butyl)ammonium iodide; ammonium chloride; acetic acid; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/chem.201002581