2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate

Base Information

Chemical Name:2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate
CAS No.:1366348-95-9
Molecular Formula:C₇H₈O₃S*C₂₂H₂₆ClN₃S
Molecular Weight:572.192
Hs Code.:

Synonyms:2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate

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Chemical Property of 2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate

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Technology Process of 2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate

There total 4 articles about 2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

: 41885-98-7
1-(4-chlorophenyl)homopiperazine

: 1037160-88-5
2-(4-chlorobutyl)benzo[d]thiazole

: 104-15-4
toluene-4-sulfonic acid

: 1366348-95-9
2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate

Guidance literature:: 1-(4-chlorophenyl)homopiperazine; 2-(4-chlorobutyl)benzo[d]thiazole; With potassium carbonate; potassium iodide; In 1,2-dimethoxyethane; for 16h; Reflux; Inert atmosphere;

toluene-4-sulfonic acid;
DOI:10.1016/j.bmc.2012.01.022

Reference yield:

: 137-07-5
2-amino-benzenethiol

: 1366348-95-9
2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 16 h / 20 °C

2: potassium carbonate; potassium iodide / 1,2-dimethoxyethane / 16 h / Reflux; Inert atmosphere

With potassium carbonate; potassium iodide; In 1,2-dimethoxyethane; toluene;
DOI:10.1016/j.bmc.2012.01.022

Reference yield:

: 637-87-6
1-Chloro-4-iodobenzene

: 1366348-95-9
2-(4-(4-(4-chlorophenyl)-1,4-diazepan-1-yl)butyl)benzo[d]thiazole tosylate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide

2: potassium carbonate; potassium iodide / 1,2-dimethoxyethane / 16 h / Reflux; Inert atmosphere

With copper(l) iodide; potassium carbonate; potassium iodide; In 1,2-dimethoxyethane;
DOI:10.1016/j.bmc.2012.01.022