Technology Process of C32H45NO6
There total 1 articles about C32H45NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-bromo-1-methoxy-2-(3-methoxypropoxy)benzene;
With
1,2-dibromobutane; iodine; magnesium;
In
tetrahydrofuran;
for 1h;
Inert atmosphere;
Reflux;
C21H29NO3;
With
cerium(III) chloride;
In
tetrahydrofuran;
at -78 ℃;
for 2h;
With
acetic acid;
In
tetrahydrofuran;
at -78 ℃;
Product distribution / selectivity;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; hydrogen; acetic acid / platinum(IV) oxide / water / 3 h / 20 °C / 760.05 Torr
2.1: sodium hydroxide; water / ethanol / 3 h / 50 °C
2.2: 20 °C
2.3: pH 1 - 2
3.1: triethylamine; 2-hydroxypyridin / tert-butyl methyl ether / 18 h / 80 °C
4.1: hydrogen; acetic acid / palladium 10% on activated carbon / ethanol / 20 °C / 760.05 Torr
4.2: pH 10
With
2-hydroxypyridin; hydrogenchloride; water; hydrogen; acetic acid; triethylamine; sodium hydroxide;
platinum(IV) oxide; palladium 10% on activated carbon;
In
ethanol; tert-butyl methyl ether; water;
- Guidance literature:
-
With
hydrogenchloride; hydrogen; acetic acid;
platinum(IV) oxide;
In
water;
at 20 ℃;
for 3h;
under 760.051 Torr;