benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Base Information

Chemical Name:benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate
CAS No.:158183-40-5
Molecular Formula:C₂₅H₂₄O₈
Molecular Weight:452.461
Hs Code.:

Synonyms:benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

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Chemical Property of benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

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Technology Process of benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

There total 9 articles about benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 158183-39-2
4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoic acid

: 158183-40-5
benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Guidance literature:: With sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 12h; Ambient temperature;

Reference yield:

: 34874-90-3
methyl haematommate

: 158183-40-5
benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Guidance literature:: Multi-step reaction with 8 steps

1: 83 percent / K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

2: 85-90percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

3: 84 percent / K₂CO₃ / acetone / 22 h / Heating

4: 85 percent / H₂ / 10percent Pd/C / ethyl acetate / 12 h / Ambient temperature

5: 61 percent / trifluoroacetic anhydride / toluene / 24 h / Ambient temperature

6: 84 percent / K₂CO₃ / dimethylsulfoxide / 14 h / Ambient temperature

7: 95 percent / H₂ / 10percent Pd/C / ethyl acetate / 12 h / Ambient temperature

8: 80 percent / NaHCO₃ / dimethylformamide / 12 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 72935-22-9
bis(benzyloxy)-2,4-formyl-3-methyl-6-benzoate de methyle

: 158183-40-5
benzyl 4-hydroxy-2-(3'-hydroxy-2'-methoxy-4'-methoxycarbonyl-5'-methylphenoxy)-6-methylbenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 85-90percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 2 h / Ambient temperature

2: 84 percent / K₂CO₃ / acetone / 22 h / Heating

3: 85 percent / H₂ / 10percent Pd/C / ethyl acetate / 12 h / Ambient temperature

4: 61 percent / trifluoroacetic anhydride / toluene / 24 h / Ambient temperature

5: 84 percent / K₂CO₃ / dimethylsulfoxide / 14 h / Ambient temperature

6: 95 percent / H₂ / 10percent Pd/C / ethyl acetate / 12 h / Ambient temperature

7: 80 percent / NaHCO₃ / dimethylformamide / 12 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;