3-N-benzoyl-3',5'-di-O-benzoyl-2'-fluoro-2'-deoxy-5-(4-tert-butyldimethylsilyloxybutyl)-1-β-D-arabinofuranosyluracil

Base Information

Chemical Name:3-N-benzoyl-3',5'-di-O-benzoyl-2'-fluoro-2'-deoxy-5-(4-tert-butyldimethylsilyloxybutyl)-1-β-D-arabinofuranosyluracil
CAS No.:1058146-44-3
Molecular Formula:C₄₀H₄₅FN₂O₉Si
Molecular Weight:744.889
Hs Code.:

Synonyms:3-N-benzoyl-3',5'-di-O-benzoyl-2'-fluoro-2'-deoxy-5-(4-tert-butyldimethylsilyloxybutyl)-1-β-D-arabinofuranosyluracil

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Chemical Property of 3-N-benzoyl-3',5'-di-O-benzoyl-2'-fluoro-2'-deoxy-5-(4-tert-butyldimethylsilyloxybutyl)-1-β-D-arabinofuranosyluracil

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Technology Process of 3-N-benzoyl-3',5'-di-O-benzoyl-2'-fluoro-2'-deoxy-5-(4-tert-butyldimethylsilyloxybutyl)-1-β-D-arabinofuranosyluracil

There total 1 articles about 3-N-benzoyl-3',5'-di-O-benzoyl-2'-fluoro-2'-deoxy-5-(4-tert-butyldimethylsilyloxybutyl)-1-β-D-arabinofuranosyluracil which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 89043-32-3
(4-bromobutoxy)-tert-butyldimethylsilane

: 157428-24-5
1-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-N³-benzoyl-5-iodouracil

: 1058146-44-3
3-N-benzoyl-3',5'-di-O-benzoyl-2'-fluoro-2'-deoxy-5-(4-tert-butyldimethylsilyloxybutyl)-1-β-D-arabinofuranosyluracil

Guidance literature:: (4-bromobutoxy)-tert-butyldimethylsilane; With iodine; zinc; In N,N-dimethyl acetamide; at 80 ℃; Inert atmosphere;

1-(3,5-di-O-benzoyl-2-deoxy-2-fluoro-β-D-arabinofuranosyl)-N³-benzoyl-5-iodouracil; With bis(tri-t-butylphosphine)palladium⁽⁰⁾; In N,N-dimethyl acetamide; at 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jm800501d