4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

Base Information

Chemical Name:4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside
CAS No.:503178-37-8
Molecular Formula:C₁₆H₁₇BrO₆
Molecular Weight:385.211
Hs Code.:

Synonyms:4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

Suppliers and Price of 4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

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Technology Process of 4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

There total 4 articles about 4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 106-41-2
4-bromo-phenol

: 3,4,6-tri-O-acetyl-D-glucal

: 503178-37-8
4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With aluminium(III) triflate; In dichloromethane; at -20 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1039/c2ob25540e

Reference yield: 52.0%

: 106-41-2
4-bromo-phenol

: 2873-29-2,3685-88-9,4098-06-0,6586-65-8,52485-06-0,63640-41-5,86257-90-1,86257-91-2,87335-77-1,87335-78-2,130931-60-1
3,4,6-tri-O-acetyl-D-glucal

: 503178-37-8
4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With Fe₃O₄(at)C-SO₃H; In 1,2-dichloro-ethane; at 80 ℃; for 2h; Green chemistry;
DOI:10.1055/s-0036-1588891

Reference yield:

: 106-41-2
4-bromo-phenol

: 2873-29-2
D-glucal triacetate

: 503178-37-8
4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enopyranoside

: 4-bromophenyl 4, 6-di-O-acetyl-2,3-dideoxy-β-D-erythro-hex-2-enopyranoside

Guidance literature:: With Fe(III) immobilized on Fe₃O₄ nanoparticles-coated carbon shell; In 1,2-dichloro-ethane; at 25 ℃; for 0.166667h; Overall yield = 74percent; Green chemistry;
DOI:10.1055/s-0037-1611855