14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane

Base Information

Chemical Name:14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane
CAS No.:75526-61-3
Molecular Formula:C₂₀H₂₈OS₂Se
Molecular Weight:427.534
Hs Code.:

Synonyms:14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane

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Technology Process of 14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane

There total 2 articles about 14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 5707-04-0
Phenylselenyl chloride

: 68872-25-3
1-[((Z)-2-But-2-enyl)-[1,3]dithian-2-yl]-cyclohexanol

: 75526-61-3
14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane

Guidance literature:: In dichloromethane; at -78 ℃;
DOI:10.1016/S0040-4020(01)93285-5 DOI:10.1021/ja00531a020

Reference yield:

: 64899-10-1
crotyldithiane

: 75526-61-3
14-(1-Phenylselanyl-ethyl)-13-oxa-1,5-dithia-dispiro[5.0.5.3]pentadecane

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / n-butyllithium / tetrahydrofuran; hexane / -78 °C

2: 83 percent / CH₂Cl₂ / -78 °C

With n-butyllithium; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja00531a020