1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate

Base Information

Chemical Name:1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate
CAS No.:1351530-51-2
Molecular Formula:C₃₅H₃₃N₂O₄*ClO₄
Molecular Weight:645.109
Hs Code.:

Synonyms:1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate

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Chemical Property of 1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate

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Technology Process of 1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate

There total 3 articles about 1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 131543-46-9,107-22-2
Glyoxal

: 73473-95-7
(2R,4S,5S)-5-amino-2,4-diphenyl-1,3-dioxacyclohexane

: 1351530-51-2
1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate

Guidance literature:: With formaldehyd; perchloric acid; In water; toluene; Inert atmosphere;
DOI:10.1016/j.jorganchem.2011.04.001

Reference yield:

: 100-52-7
benzaldehyde

: 1351530-51-2
1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentoxide / 18 h / 20 °C / Inert atmosphere

2: formaldehyd; perchloric acid / water; toluene / Inert atmosphere

With formaldehyd; perchloric acid; phosphorus pentoxide; In water; toluene;
DOI:10.1016/j.jorganchem.2011.04.001

Reference yield:

: 73473-94-6
(1S,2S)-(+)-2-Amino-1-phenyl-1,3-propandiol-hydrobromid

: 1351530-51-2
1,3-di-[(2R,4S,5S)-2,4-diphenyl-1,3-dioxacyclohex-5-yl]imidazolium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus pentoxide / 18 h / 20 °C / Inert atmosphere

2: formaldehyd; perchloric acid / water; toluene / Inert atmosphere

With formaldehyd; perchloric acid; phosphorus pentoxide; In water; toluene;
DOI:10.1016/j.jorganchem.2011.04.001