C₂₄H₄₀BrNO₅Si

Base Information

Chemical Name:C₂₄H₄₀BrNO₅Si
CAS No.:1571933-82-8
Molecular Formula:C₂₄H₄₀BrNO₅Si
Molecular Weight:530.575
Hs Code.:

C<sub>24</sub>H<sub>40</sub>BrNO<sub>5</sub>Si

Synonyms:C₂₄H₄₀BrNO₅Si

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Chemical Property of C₂₄H₄₀BrNO₅Si

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Technology Process of C₂₄H₄₀BrNO₅Si

There total 7 articles about C₂₄H₄₀BrNO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1571933-96-4
C₂₇H₄₉NO₅SiSn

: 1571933-82-8
C₂₄H₄₀BrNO₅Si

Guidance literature:: With bromine; In methanol; diethyl ether; at -70 ℃; for 0.5h;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1571933-82-8
C₂₄H₄₀BrNO₅Si

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / water; 1,4-dioxane / -2 - 0 °C

2: N,N-dimethylformamide dineopentyl acetal / toluene / 3 h / Reflux

3: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

4: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride / toluene / 6 h / 100 °C / Inert atmosphere

6: bromine / methanol; diethyl ether / 0.5 h / -70 °C

With 1H-imidazole; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; iodine; silver trifluoroacetate; triethylamine; N,N-dimethylformamide dineopentyl acetal; lithium chloride; In 1,4-dioxane; methanol; diethyl ether; chloroform; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1571933-49-7
C₂₄H₄₁NO₅Si

: 1571933-82-8
C₂₄H₄₀BrNO₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: silver trifluoroacetate; iodine / chloroform / 120 h / -60 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; lithium chloride / toluene / 6 h / 100 °C / Inert atmosphere

3: bromine / methanol; diethyl ether / 0.5 h / -70 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; iodine; silver trifluoroacetate; lithium chloride; In methanol; diethyl ether; chloroform; toluene;