2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene
CAS No.:1083009-44-2
Molecular Formula:C₁₉H₁₇BF₂I₂N₂
Molecular Weight:575.974
Hs Code.:

Synonyms:2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

Suppliers and Price of 2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 9 raw suppliers

Chemical Property of 2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

Chemical Property:

Melting Point:194.3-194.9 °C

Purity/Quality:: 99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

There total 10 articles about 2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: phenyl BODIPY

: 1083009-44-2
2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With iodine; iodic acid; In tetrahydrofuran; ethanol; Inert atmosphere;
DOI:10.1002/pola.28902

Reference yield: 91.0%

: 7553-56-2,12190-71-5,8031-47-8
iodine

: phenyl BODIPY

: 1083009-44-2
2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With iodic acid; In ethanol; dichloromethane; water; at 60 ℃; for 2h;
DOI:10.1016/j.bmc.2013.07.017

Reference yield:

: 98-88-4
benzoyl chloride

: 1083009-44-2
2,6-diiodo-4,4-difluoro-1,3,5,7-tetramethyl-8-phenyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 20 °C / Inert atmosphere

1.2: 1 h / Inert atmosphere; Cooling with ice

2.1: N-iodo-succinimide / dichloromethane / 0.5 h / 20 °C

With N-iodo-succinimide; In dichloromethane;
DOI:10.1021/jo200990y