2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide

Base Information

Chemical Name:2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide
CAS No.:859537-26-1
Molecular Formula:C₁₇H₂₃N₃OS
Molecular Weight:317.455
Hs Code.:

2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1<i>H</i>-imidazol-2-ylsulfanyl]-acetamide

Synonyms:2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide

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Chemical Property of 2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide

Chemical Property:

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Technology Process of 2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide

There total 4 articles about 2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 859537-17-0
4-(3,5-dimethyl-benzyl)-5-isopropyl-1,3-dihydro-imidazole-2-thione

: 144-48-9
iodacetamide

: 859537-26-1
2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide

Guidance literature:: 4-(3,5-dimethyl-benzyl)-5-isopropyl-1,3-dihydro-imidazole-2-thione; With potassium hydroxide; In methanol; at 20 ℃; for 0.5h;

iodacetamide; In methanol; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2005.04.024

Reference yield:

: 859537-05-6
N-[1-(3,5-dimethyl-benzyl)-3-methyl-2-oxo-butyl]-isobutyramide

: 859537-26-1
2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 80 percent / hydrochloric acid / ethanol / 10 h / Heating

2.1: 84 percent / H₂O / 3 h / Heating

3.1: potassium hydroxide / methanol / 0.5 h / 20 °C

3.2: 52 percent / methanol / 1 h / 20 °C

With hydrogenchloride; potassium hydroxide; In methanol; ethanol; water;
DOI:10.1016/j.bmc.2005.04.024

Reference yield:

: 2-amino-1-(3,5-dimethylbenzyl)-4-methyl-pentan-3-one hydrochloride

: 859537-26-1
2-[5-(3,5-dimethyl-benzyl)-4-isopropyl-1H-imidazol-2-ylsulfanyl]-acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 84 percent / H₂O / 3 h / Heating

2.1: potassium hydroxide / methanol / 0.5 h / 20 °C

2.2: 52 percent / methanol / 1 h / 20 °C

With potassium hydroxide; In methanol; water;
DOI:10.1016/j.bmc.2005.04.024